Replicated Grazing Incidence X-Ray Optics 
  René Hudec, Ladislav Pína, Adolf Inneman 
ABSTRACT

The replication technology represents an important alternative to other methods of X-ray optics production. We report on the past (first replicated X-ray mirror has been produced by our group just 30 years ago), present and future of replication of X-ray optics with emphasis on grazing incidence optics of various types and geometry. The various types of X-ray optics produced by replication with emphasis on astronomical optics are described and summarized. It is shown that the replicated X-ray optics will still play a major role in future space experiments and projects such as the ESA XEUS project and other coming missions.

INTRODUCTION

Major scientific achievements of the last two decades of X-ray astronomy are closely related to the use of imaging X-ray telescopes. These telescopes achieve much better signal/noise ratio than X-ray experiments without optics - this allows e.g. the detection of faint sources. The use of X-ray optics further allows imaging, precice localization, photometry, spectroscopy, variability studies, and estimation of physical parameters of X-ray emitting regions (temperature, electron density...).

The space experiments with X-ray optics are also well suited for monitoring of X-ray sky for variable and transient objects including X-ray novae, X-ray transients, X-ray flares on stars and AGNs, galactic bulge sources, X-ray binaries, SGRs (Soft Gamma Ray Repeaters) and X-ray afterglows of GRBs (Gamma Ray Bursts). The X-ray optics represent an important part of numerous past, recent, and future space projects (EXOSAT, ROSAT, Einstein, RT-4M Salyut 7, Fobos, AXAF, XMM, ABRIXAS, BeppoSAX, ASCA, XEUS...). In the laboratory, there are numerous applications of the X-ray optics e.g. in plasma physics, laser plasma, biology, crystallography, medicine, etc.

fig1

Fig. 1: Replicated grazing incidence X-ray optics
THE VARIOUS TYPES OF X-RAY OPTICS

According to the physical processes involved, one can divide the X-ray optics into the following groups:

  • diffractive optics (Fresnel lenses + pinholes): not useful for space due to small apertures
  • refractive optics: limited use, not useful for space
  • reflective optics, based on total reflection (grazing incidence)
  • reflective optics, allowing normal incidence (multilayers)
  • In this paper, we will concentrate on reflective X-ray lenses (mirrors).

    Wolter optics: The Wolter type optics is in wide use in space-borne X-ray astronomical experiments (ROSAT, EXOSAT, Salyut 7, Fobos, XMM, AXAF..). It is based on double reflection on two surfaces (requirement for a superior imaging - the Abbe sine condition). Depending on the combination of surfaces, there are various modifications (Wolter I, II, III types), mostly used is the Wolter I type (paraboloid + hyperboloid).

    Double-cone approximation of Wolter optics: The Wolter surfaces can be approximated by less laborious and hence less expensive conical profiles. These mirrors have lower imaging quality but in many cases larger collecting area since the conical shells can be made very thin. These mirrors usually represent high throughput systems, and can be preferably used in foil telescopes (SODART).

    Conical, ellipsoidal and paraboloidal optics: These mirrors with only one reflection find most of their applications in the laboratotry either as collimating or focussing and/or imaging elements.

    Kirkpatrick-Baez optics: This configuration is used mostly in experiments not requiring large collecting area (solar, laboratory). Recently, large modules of KB mirrors have been suggested also for stellar X-ray experiments.

    Normal incidence optics: This optics requires the multilayer deposition on the mirror surface allowing its use under normal incidence. The use of multilayers results in narrow spectral range, and in the past has been used mostly in solar experiments (TEREK Fobos, TEREK KORONAS...) as well as in laboratory applications.

    Lobster-eye optics: This optics has been suggested in 70ies for very wide field X-ray imaging but not yet used in space mostly due to severe manufacturing problems. Recently, the first test modules are available for both the Schmidt as well as for the alternative Angel configurations.

    The development and manufacture of various types of reflective X-ray optics are heavily affected by manufacturing problems, making their production laborious and hence expensive. The most dominating problems can be summarized as follows: (1) the required microroughness is less than 3 nm, in many applications however less than 1 nm, (2) the X-ray optics is frequently represented by hollow inner surfaces, and (3) there are very strict requirements on the slope errors and shape deviations.

    THE REPLICATED X-RAY OPTICS

    1. Early Stages

    The early stages of the X-ray optics developments in the Czech Republic are closely related to the INTERKOSMOS Space Programme (Soviet and East European equivalent of ESA operated until 1989). All of the X-ray imaging telescopes onboard Soviet spacecrafts were equipped with the Czech X-ray optics (exception: X-ray normal incidence mirrors in the special channel of the TEREK telescopes onboard the Fobos and Koronas spacecrafts). Later on, also the laboratory applications have started. In almost all cases, replicated grazing incidence mirrors of various geometries, types and arrangements have been designed and developed. The replication technology proved to be powerful tool in solving numerous and various different problems and demands.

    fig2
    Fig. 2: First X-ray images of the Sun obtained on X-ray film, Vertikal 9 rocket, 1979
    fig3
    Fig. 3: The three inner channels (from left to right: EUV channel, X channel, coronagraph channel) of the TEREK X-ray telescope and coronagraph, Fobos 1 spacecraft, 1988.


    fig4
    Fig. 4: The assembled TEREK experiment.
  • 1969 first considerations started
  • 1970 first X-ray mirror produced (Wolter 1, 50 mm)
  • 1971 Wolter 1, 80 mm
  • 1976 Wolter 1, 115 mm
  • 1979 first mirrors flown in space (two Wolter 1, 50 mm, Vertikal 9 rocket)
  • 1980 Vertikal 11 rocket (two Wolter 1, 50 mm)
  • 1981 first large Wolter 1 mirror (240 mm)
  • 1981 Salyut 7 orbital station, RT- 4M stellar X-ray telescope (Wolter 240 mm, double nested objective)
  • 1985 applications for plasma physics, EH 17 mm, PP 20 mm
  • 1987 first high quality X-ray foils for foil mirror X-ray telescope (SODART)
  • 1988 Fobos 1 Mars probe, TEREK X-Ray solar telescope
  • 1989 KORONAS I X-Ray mirror, Wolter 80 mm
  • 1990 first micromirror (aperture less than 1 mm)
  • 1993 collaboration with SAO, USA, WF X-Ray optics started
  • 1996 first Lobster Eye test module produced, Schmidt geometry
  • 1997 Lobster Eye Angel geometry project started
  • 1999 first Lobster Eye test module produced, Angel geometry
  • It is obvious that this type of X-ray wide field telescopes could play an important role in future X-ray astrophysics. The innovative very wide field X-ray telescopes have been suggested based on these optical elements but have not been flown in space so far. One of the proposals is the All Sky Supernova and Transient Explorer (ASTRE)1. This proposal also includes a cylindrical coded aperture outside of the reflectors which provide angular resolution along the cylinder axis. The coded aperture contains circumferential open slits 1 mm wide in a pseudo-random pattern.

  • Total number of X-ray mirrors produced: more than 50
  • Total number of mirrors flown in space: 8
  • Total spacecrafts with Czech X-ray optics: 4
  • Total number of space experiments with Czech X-ray optics onboard: 8
  • 2. Technologies

    The mirrors have been produced by various replication technologies:

  • 1970 Heavy Replica Technology: heavy electroforming of X-ray mirror shells from polished glass masters, wall thickness 5-10 mm
  • 1978 Replica Epoxy Technology tested: epoxy replication of gold evaporated glass masters
  • 1980 Replica Epoxy Electroforming Technology: thin electroformed shells reinforced by epoxy
  • 1981 as above but carbon fibre filling involved
  • 1982 super-thin test Wolter shells for hight throughput telescopes
  • 1983 flat master replication: production of X-ray reflecting foils for foil X-ray telescopes (SODART, RENTGEN SPEKTR GAMA)
  • 1990 first micromirrors (aperture ~ 1 mm) produced
  • 1993 first double - sided replicated flats for Lobster telescopes of Schmidt type
  • 1998 first replication of Angel geometry Lobster Eye cells
  • fig5
    Fig. 5: Microscopic X-ray mirrors (from the left to the right: EH 17 mm, PP 20 mm, Lobster test channels)
    3. Replication Technique

    The idea of replica technology is to create perfect copy of negative shaped master and of smooth surfaces. This is very suitable if the negative shape is easier to be produced.

    The two main advantages of the replication in X-ray optics design and construction are as follows:

  • the production of negative shapes is less laborious
  • the produced shells may be much thinner than is possible with classical technologies (important for light-weight high throughput nested arrays)
  • The replication by electroforming has been used in the Czech Republic for development and production of X-ray mirrors since 1967. Since then, the technology has been further developed and modified. A number of modifications exist, meeting different demands. The replication is perfectly suitable for the production of X-ray grazing incidence optics since external surfaces can be much easily grinded and polished than inner cavities (especially in the case of small apertures). The masters are of high quality optical glass, glass ceramics or metals. It should be noted that the replication technology in X-ray optics is applied by different groups in various different modifications.

    4. Characteristics

    The basic characteristics of by electroforming replicated X-ray mirrors can be summarized as follows.

  • Reflecting surfaces: electroformed Ni, or electroformed Au, or evaporated/ sputtered Au. Other materials are also possible as well as additional coatings.
  • External surface-structure: metallic (Ni), or CF/epoxy, or sandwich.
  • Parameters: the mirrors are polychromatic from 10 keV to optical wavelengths. They have a high reflectivity, up to 90% depending on the wavelength and the grazing angle (e.g. 60% at 0.83 nm and 1 deg incidence angle). The mirrors have smooth surfaces analogous to surfaces of masters. Thickness uniformity is of order of 2%.
  • Additional technologies: multilayers may also be applied to achieve better energy coverage (hard X-rays up to 100 keV). Superpolishing and/or surface quality improvements by lacquer coating are also possible.
  • 5. Advantages

    The replicated X-ray mirrors have numerous advantages which can be summarized as follows.

  • Wide variety of geometries is possible: Wolter I, II and III systems, conical, ellipsoidal, paraboloidal, flats etc.
  • Light-weight and thin shells are possible. This is important for high throughput X-ray optics (nested arrays with many shells) and for space applications in general.
  • Multiple replication of identical elements is possible, minimizing the price of final mirrors.
  • There is no need to grind and to polish small inner cavities - negative shapes are to be polished
  • There are almost no aperture limits including both very small (below 1 mm) and very large (more than 500 mm) apertures
  • There is large number of various applications
  • The surfaces are resistant to space and/or laboratory environment (cleaning possible, no heat degradation)
  • The replicated Au surfaces are more smooth than evaporated surfaces
  • 6. Summary of X-Ray Astronomical mirrors produced

    Approximately 50 mirrors have been produced between 1970 and 1999 as well as numerous tests for technology purposes:

  • Wolter 1 mirrors for space applications, apertures 40 to 240 mm. They have been used onboard satellites as imaging elements in X-ray solar and stellar telescopes
  • Bent foil mirrors/flats foils. X-ray reflecting foils produced from float glass masters with sizes up to 300 x 400 mm. Thickness homogenity better than 2%. Wide range of foil thickness from a few microns up to 1 mm. Designed for the SODART foil X-ray telescope and analogous projects.
  • Lobster-eye wide-field X-ray optics, Schmidt geometry, various modules, size of the flats 80 x 100 mm and 23 x 23 mm.
  • Lobster-eye wide-field X-ray optics, Angel geometry, various test modules, a/L (aperture/length) ratios of about 50-80.
  • 7. Summary of Laboratory Mirrors Produced

    The replication technology has also been applied in numerous ground-based and laboratory applications which are listed below.

  • PP (paraboloid-paraboloid) microscopes, aperture 20 mm
  • EH (ellipsoid-hyperboloid ) Wolter microscopes, aperture 17 mm
  • Conical, ellipsoidal, paraboloidal mirrors
  • Micromirrors of conical, ellipsoidal, and paraboloidal profiles
  • Foils including those for foil X-ray telescopes
  • Flat and bent mirrors
  • fig6 fig7
    Fig. 6, 7: The X-ray reflexivity measurements for float glass 0.3 mm thick sample covered by 20 W/Si multilayers (left) and float glass 2.3 mm thick of Czech production (Teplice) covered by C/Au layers (right).

    RECENT AND FUTURE ACTIVITIES

    1. Lobster-Eye Wide-Field X-Ray Telescopes

    The widely used Wolter objectives have a very limited FOV (typically of order of 1 degree or less) so they are suitable for pointed observations but not for monitoring and surveys. The wide-field X-ray optics has been suggested in 70ies by Schmidt (orthogonal stacks of reflectors) and by Angel (array of square cells) but has not been constructed yet. With this type of reflective X-ray optics, up to 180 deg FOV may be achieved.

    The difficult production of Lobster eye (LE) lenses has caused the significant delay between their theoretical description and their construction and real use. The possible solution is offered recently by the replication technology. Recently, the first Lobster-eye X-ray telescope prototypes have been successfully finished. The prototype of Schmidt geometry represents one module and consists of two perpendicular arrays of double-sided X-ray reflecting flats (36 and 42 double-sided flats100 x 80 mm each). The flats are 0.3 mm thick and gold-coated. The focal distance is 400 mm from the midplane. The FOV of one module is about 6.5 degrees. More such modules may create an array with substantially larger FOV.

    Improved Schmidt test modules have been finished in 1999 with aperture/length ratios of up to 80, based on 0.1 mm thick gold-coated glass plates spaced at 0.3 mm.

    fig8
    Fig. 8: Lobster-Eye telescope prototypes, Angel(in the center) and Schmidt (left and right) arrangements
    fig9
    Fig. 8: Lobster-Eye telescope prototypes, Angel(in the center) and Schmidt (left and right) arrangements

    For the Angel geometry, numerous square cells of very small size (about 1x1 mm or less at lengths of order of tens of mm) are to be produced. This is much more difficult than the Schmidt arrangement mentioned above. Nevertheless, the recent results indicate that this demand can be also solved by modified innovative replication technology.

    Three test Angel LE modules have been produced so far: (1) a linear module with 47 cells of 2.5 x 2.5 mm 120 mm long, f = 1.3 m, (2) a 2D module with 6 x 6 cells, dimensions and f as above, surface microroughness 0.8 nm, and (3) a L-shaped module of 2 x 18 cells with parameters as above. Another LE Angel test module is in development: 2D module with 96 x 96 = 9 216 cells 2.5 x 2.5 mm, 120 mm long, f = 1.3 m.

    The LE X-ray telescopes are extremely important since the discovery of X-ray afterglows of Gamma Ray Burst (GRBs) sources in 1997. The expected rate of GRBs is 1 per day, however the theoretical prediction assumes larger beaming angle in X-rays if compared with gamma rays, hence the actual rate of X-ray afterglows is expected to be substantially larger (nearly 10 x or even more) than the rate of GRBs, hence about 10 X-ray afterglows are expected daily.

    The sensitivity of LE telescopes is sufficient enough to detect the recently discovered X-ray GRB afterglows. It should be also noted that the localization accuracy of the LE telescopes is of order of 1 arcmin, substantially exceeding the recent localization accuracy of most gamma ray instruments (2 deg and more). It is hence obvious that the LE telescopes are expected to provide a substantial contribution to the science and statistics of GRBs. The additional science of LE X-ray telescopes includes supernova explosions, high energy binary sources, AGNs, blazars, X-ray novae, X-ray transients etc.

    fig10
    Fig. 8: Lobster-Eye telescope prototypes, Angel(in the center) and Schmidt (left and right) arrangements
    2. Laboratory X-Ray Optics

    Numerous applications exist for the replicated reflective X-ray optics e.g. in the plasma physics, nuclear fusion, biology, crystallography etc. with various geometries and arrangements with apertures below 20 mm and, in some cases, even below 1 mm6. Examples: micromirrors, PP systems, EH systems, Wolter mirrors, X-ray microscopes. Recently, micromirrors are in development for the X-ray laboratory experiment onboard the International Space Station / SS (protein crystallography).

    fig11 fig12
    Fig. 11: X-ray micromirror Fig. 12: X-ray reflectivity measurement of X-ray micromirror
    fig13 fig14
    Fig. 13, 14: Microroughness measurements of various mandrel and replica test surfaces
    DISCUSSION

    The (replicated) grazing incidence X-ray optics shows some advantages if compared with other types of X-ray imaging and focussing elements which can be summarized as follows:

  • Wide energy range (no narrow window)
  • Large collecting area
  • Resistant to heat and other environment influences
  • High reflectivity, over 90% depending on the grazing angle
  • Wide field systems are possible
  • Cost-effective production
  • Arrangements are possible which could hardly be effectively produced by classical methods such as thin and multiple shells, multiple and nested arrays etc.
  • The grazing incidence X-ray optics is in use within space experiments already for 30 years. Despite of this, some innovative types of the X-ray mirrors are still in the development phase. Moreover, the requirements for future missions are much higher than for those in the past so new and innovative technologies are necessary. The future of astronomical grazing incidence X-ray optics can be briefly summarized as follows:

  • segmented large aperture mirrors (e.g. XEUS)
  • high throughput optics/very thin shells
  • wide field imaging systems, FOV >> 1 deg
  • better surface quality (less than 1 nm), reduced slope errors, arcsec angular resolution, new technologies
  • better spectral coverage - multilayers and other additional layers, imaging in hard X-rays up to 100 keV
  • For laboratory applications, improved imaging quality and superior angular resolution (X-ray microscopes) are required. These needs require innovative technologies for the future:

  • superpolishing: to achieve superior angular resolution and high efficiency
  • application and/or replication of multilayers: to achieve a better spectral coverage (for hard X-rays, up to 100 keV)
  • improving the surface quality: to achieve superior angular resolution and high efficiency
  • innovative measuring techniques
  • very large apertures: to achieve high detection sensitivity
  • very wide-field of view systems: to achieve WF X-ray monitoring of the sky
  • very large collecting areas: to achieve high sensitivity
  • ACKNOWLEDGEMENTS

    The development of innovative X-ray telescopes is supported by the grant 105/99/1546 provided by the Grant Agency of the Czech Republic. We further acknowledge the support provided by the ROTAN Laboratory, Physical Institute of the Academy of Sciences of the Czech Republic (X-ray reflectivity measurements), by the Optical Development Workshop of the Academy of Sciences of the Czech Republic (mandrels developments and production), by the X-ray Astronomy group at the University of Leicester, UK and Reflex Prague (X-ray tests of LE telescopes), by the TTS Prague (gold-coating), by the Astronomical Observatory Brera, Italy (microroughness AFM measurements), and by the Physical Institute of the Slovak Academy of Sciences, Piestany (multilayer deposition).

    REFERENCES

  • 1. H. Wolter, Ann. Der Phys. 10, 94, 1952.
  • 2. P. Gorenstein: Proc. Symposium X-ray surveys, Potsdam, 1998.
  • 3. W. K. H. Schmidt, Nucl. Instr. Methods, 127, 285-292, 1975.
  • 4. J. R. P. Angel, ApJ, 233, 364-373, 1979.
  • 5. R. Hudec, A. Inneman, L. Pina : this volume, 2000.
  • 6. L. Pína, A. Inneman, R. Hudec: Proc. SPIE 3766 "X-ray Optics, Instruments and Missions II",Ed. R. B. Hoover and A. B. Walker, 2000, in press.

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